(S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid

Base Information

• Chemical Name: (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid
• CAS No.: 184107-25-3
• Molecular Formula: C₃₁H₃₀N₂O₄
• Molecular Weight: 494.59

Synonyms:(S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid

Chemical Property of (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid

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Technology Process of (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid

There total 3 articles about (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

methyl (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]-cyclohepten-5-ylidene)piperidin-1-yl]propionate (184107-20-8) → (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid (184107-25-3)

Guidance literature:

With sodium hydroxide; In ethanol; water; for 3h; Ambient temperature;

DOI:10.1016/S0223-5234(97)87535-6

Reference yield:

4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidine (14051-46-8) → (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid (184107-25-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 49 percent / NaI, Na₂CO₃ / acetone / Heating

2: 91 percent / NaOH / ethanol; H₂O / 3 h / Ambient temperature

With sodium hydroxide; sodium carbonate; sodium iodide; In ethanol; water; acetone;

DOI:10.1016/S0223-5234(97)87535-6

Reference yield:

2-Benzyloxycarbonylamino-3-chloro-propionic acid methyl ester → (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidin-1-yl]propionic acid (184107-25-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 49 percent / NaI, Na₂CO₃ / acetone / Heating

2: 91 percent / NaOH / ethanol; H₂O / 3 h / Ambient temperature

With sodium hydroxide; sodium carbonate; sodium iodide; In ethanol; water; acetone;

DOI:10.1016/S0223-5234(97)87535-6

upstream raw materials:

methyl (S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]-cyclohepten-5-ylidene)piperidin-1-yl]propionate

4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidine

Downstream raw materials:

Ethyl α-{(S)-2-benzyloxycarbonylamino-3-[4-(5H-dibenzo[a,d]-cyclohepten-5-ylidene)piperidine-1-yl]propionylamino}acetate

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