O,O-diethyl 1-((4,6-dichloropyrimidin-2-yl)carbamyloxy)-1-(4-chlorophenyl)methylphosphonate

Base Information

Chemical Name:O,O-diethyl 1-((4,6-dichloropyrimidin-2-yl)carbamyloxy)-1-(4-chlorophenyl)methylphosphonate
CAS No.:1614827-44-9
Molecular Formula:C₁₆H₁₇Cl₃N₃O₅P
Molecular Weight:468.661
Hs Code.:

Synonyms:O,O-diethyl 1-((4,6-dichloropyrimidin-2-yl)carbamyloxy)-1-(4-chlorophenyl)methylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O,O-diethyl 1-((4,6-dichloropyrimidin-2-yl)carbamyloxy)-1-(4-chlorophenyl)methylphosphonate

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Technology Process of O,O-diethyl 1-((4,6-dichloropyrimidin-2-yl)carbamyloxy)-1-(4-chlorophenyl)methylphosphonate

There total 2 articles about O,O-diethyl 1-((4,6-dichloropyrimidin-2-yl)carbamyloxy)-1-(4-chlorophenyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108054-54-2,20641-28-5
diethyl (4-chlorophenyl)(hydroxy)methylphosphonate

: 59376-71-5
4,6-dichloro-2-pyrimidinyl isocyanate

: 1614827-44-9
O,O-diethyl 1-((4,6-dichloropyrimidin-2-yl)carbamyloxy)-1-(4-chlorophenyl)methylphosphonate

Guidance literature:: In 1,2-dichloro-ethane; at 20 ℃; for 0.25h;
DOI:10.1080/10426507.2013.855774

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1614827-44-9
O,O-diethyl 1-((4,6-dichloropyrimidin-2-yl)carbamyloxy)-1-(4-chlorophenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine

2: 1,2-dichloro-ethane / 0.25 h / 20 °C

With triethylamine; In 1,2-dichloro-ethane;
DOI:10.1080/10426507.2013.855774