2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole

Base Information

Chemical Name:2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole
CAS No.:896445-16-2
Molecular Formula:C₃₀H₂₈Br₂N₄O₂
Molecular Weight:636.386
Hs Code.:

Synonyms:2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole

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Chemical Property of 2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole

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Technology Process of 2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole

There total 6 articles about 2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 896445-18-4
C₃₀H₃₂Br₂N₄O₄

: 896445-16-2
2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole

Guidance literature:: With trichlorophosphate; at 90 ℃;
DOI:10.1039/b517067b

Reference yield:

: 13731-82-3
2,5-dibromoterephtalic acid

: 896445-16-2
2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / 4 h / Heating

2: 2.1 g / 4 h / Heating

3: 95 percent / hydrazine monohydrate / methanol / Heating

4: 73 percent / pyridine / 12 h

5: 70 percent / POCl₃ / 90 °C

With pyridine; thionyl chloride; hydrazine hydrate; trichlorophosphate; In methanol;
DOI:10.1039/b517067b

Reference yield:

: 1074-24-4
2,5-dibromo-p-xylene

: 896445-16-2
2-(4-tert-butylphenyl)-5-(2,5-dibromo-4-(5-(4-tertbutylphenyl)-1,3,4-oxadiazol-2-yl)phenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide; potassium permanganate / H₂O / 12 h / Heating

2: SOCl₂ / 4 h / Heating

3: 2.1 g / 4 h / Heating

4: 95 percent / hydrazine monohydrate / methanol / Heating

5: 73 percent / pyridine / 12 h

6: 70 percent / POCl₃ / 90 °C

With pyridine; sodium hydroxide; potassium permanganate; thionyl chloride; hydrazine hydrate; trichlorophosphate; In methanol; water;
DOI:10.1039/b517067b