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Technology Process of [(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)](1+)*Cl(1-)=[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)]Cl

[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)](1+)*Cl(1-)=[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)]Cl

Base Information
  • Chemical Name:[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)](1+)*Cl(1-)=[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)]Cl
  • CAS No.:1072314-63-6
  • Molecular Formula:C23H25ClNOTi*Cl
  • Molecular Weight:450.244
  • Hs Code.:
[(C<sub>5</sub>H<sub>5</sub>)TiCl(C<sub>5</sub>H<sub>4</sub>C(CH<sub>2</sub>)4CH<sub>2</sub>C(O)NHC<sub>6</sub>H<sub>5</sub>)]<sup>(1+)</sup>*Cl<sup>(1-)</sup>=[(C<sub>5</sub>H<sub>5</sub>)TiCl(C<sub>5</sub>H<sub>4</sub>C(CH<sub>2</sub>)4CH<sub>2</sub>C(O)NHC<sub>6</sub>H<sub>5</sub>)]Cl

Synonyms:[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)](1+)*Cl(1-)=[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)]Cl

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Chemical Property of [(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)](1+)*Cl(1-)=[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)]Cl
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Technology Process of [(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)](1+)*Cl(1-)=[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)]Cl

There total 1 articles about [(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)](1+)*Cl(1-)=[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

thionyl chloride
7719-09-7

thionyl chloride

[(C<sub>5</sub>H<sub>5</sub>)TiCl(C<sub>5</sub>H<sub>4</sub>C(CH<sub>2</sub>)4CH<sub>2</sub>CO<sub>2</sub>)]
1072315-26-4

[(C5H5)TiCl(C5H4C(CH2)4CH2CO2)]

aniline
62-53-3

aniline

[(C<sub>5</sub>H<sub>5</sub>)TiCl(C<sub>5</sub>H<sub>4</sub>C(CH<sub>2</sub>)4CH<sub>2</sub>C(O)NHC<sub>6</sub>H<sub>5</sub>)]<sup>(1+)</sup>*Cl<sup>(1-)</sup>=[(C<sub>5</sub>H<sub>5</sub>)TiCl(C<sub>5</sub>H<sub>4</sub>C(CH<sub>2</sub>)4CH<sub>2</sub>C(O)NHC<sub>6</sub>H<sub>5</sub>)]Cl
1072314-63-6

[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)](1+)*Cl(1-)=[(C5H5)TiCl(C5H4C(CH2)4CH2C(O)NHC6H5)]Cl

Guidance literature:
With NaH; In dichloromethane; Ti complex was reacted with SOCl2 at room temp. for 1 h; heated at 50°C for 2 h in vac.; dissolved in CH2Cl2; transferred to suspn. of NaH and aniline in CH2Cl2; stirred at room temp. for 16 h; filtered through Celite; crystd. (CH2Cl2/pentane);
DOI:10.1021/om800700c
upstream raw materials:

thionyl chloride

[(C5H5)TiCl(C5H4C(CH2)4CH2CO2)]

aniline

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