C₄₁H₆₆O₆Si₂

Base Information

Chemical Name:C₄₁H₆₆O₆Si₂
CAS No.:1268455-97-5
Molecular Formula:C₄₁H₆₆O₆Si₂
Molecular Weight:711.142
Hs Code.:

C<sub>41</sub>H<sub>66</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₄₁H₆₆O₆Si₂

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Chemical Property of C₄₁H₆₆O₆Si₂

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Technology Process of C₄₁H₆₆O₆Si₂

There total 27 articles about C₄₁H₆₆O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1268455-83-9
C₃₅H₅₂O₆Si

: 69739-34-0
t-butyldimethylsiyl triflate

: 1268455-97-5
C₄₁H₆₆O₆Si₂

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1021/ol1031409

Reference yield: 100.0%

: 1268455-83-9
C₃₅H₅₂O₆Si

: 1268455-97-5
C₄₁H₆₆O₆Si₂

Guidance literature:: With 2,6-dimethylpyridine; t-butyldimethylsiyl triflate; In dichloromethane; at 0 ℃;
DOI:10.1246/bcsj.20120152

Reference yield:

: 1268455-52-2
C₂₄H₃₈O₄Si

: 1268455-97-5
C₄₁H₆₆O₆Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: methanol; camphor-10-sulfonic acid / dichloromethane / 12 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 14.5 h / 50 °C

5.1: methanol; camphor-10-sulfonic acid / dichloromethane / 2 h / 0 °C

6.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 0.5 h / 0 °C

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 20 °C

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; hexamethyldistannane; lithium chloride / tetrahydrofuran / 1.5 h / 70 °C

9.2: 3.5 h / 20 °C

10.1: zinc borohydride / diethyl ether / 24 h / -40 °C

11.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-methyl-but-2-ene; zinc borohydride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hexamethyldistannane; sulfur trioxide pyridine complex; sodium hydride; triethylamine; dicyclohexyl-carbodiimide; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;
DOI:10.1021/ol1031409