N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide

Base Information

• Chemical Name: N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide
• CAS No.: 133689-52-8
• Molecular Formula: C₃₈H₃₈N₂O₄
• Molecular Weight: 586.731

Synonyms:N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide

Chemical Property of N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide

Chemical Property:

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Technology Process of N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide

There total 4 articles about N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2,6-diisopropylbenzenamine (24544-04-5) + 1,4,5,8-naphthalenetetracarboxylic dianhydride (81-30-1) → N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide (133689-52-8)

Guidance literature:

In acetic acid; for 16h; Reflux;

DOI:10.1021/jacs.9b12328

Reference yield: 82.0%

→ N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide (133689-52-8)

Guidance literature:

In ethanol; for 2h; Reflux; Inert atmosphere;

Reference yield: 13.0%

2,6-diisopropylbenzenamine (24544-04-5) + 1,4,5,8-naphthalenetetracarboxylic dianhydride (81-30-1) → N,N‘-(di-2,6-diisopropylphenyl)naphthalene-1,4,5,8,-tetracarboxylic acid bisimide (133689-52-8) + N-(2,6-diisopropylphenyl)-1,4,5,8,-naphthalentetracarboxylic acid 1,8-anhydride-4,5-imide (1613023-61-2)

Guidance literature:

In N,N-dimethyl-formamide; at 165 ℃; for 12h;

DOI:10.1039/c5cc07238g

upstream raw materials:

2,6-diisopropylbenzenamine

1,4,5,8-naphthalenetetracarboxylic dianhydride

Downstream raw materials:

C₄₆H₅₂N₄O₄

C₄₂H₄₅N₃O₄

C₄₃H₄₇N₃O₄

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