Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Base Information

Chemical Name:Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester
CAS No.:179984-38-4
Molecular Formula:C₂₇H₃₀INO₆S
Molecular Weight:623.509
Hs Code.:

Synonyms:Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

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Chemical Property of Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

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Technology Process of Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

There total 4 articles about Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-19-7
propargyl alcohol

: octanedioic acid mono-(2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl) ester

: 179984-38-4
Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Guidance literature:: With triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(00)00660-8

Reference yield:

: 144863-34-3
3-(2'-iodo-N-phenylsulphonylanilinyl)-2-chloromethylpropene

: 179984-38-4
Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaOAc / dimethylformamide / 48 h / 80 °C

1.2: 78 percent / HCl / methanol / 24 h / 20 °C

2.1: DMAP; DCC / dimethylformamide / 12 h / 20 °C

3.1: triphenylphosphine; ADDP / tetrahydrofuran / 24 h / 20 °C

With dmap; sodium acetate; dicyclohexyl-carbodiimide; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: Substitution / 1.2: Hydrolysis / 2.1: Etherification / 3.1: Etherification;
DOI:10.1016/S0040-4020(00)00660-8

Reference yield:

: sodium N-(2-iodophenyl)phenylsulfonamide

: 179984-38-4
Octanedioic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylformamide / 24 h

2.1: NaOAc / dimethylformamide / 48 h / 80 °C

2.2: 78 percent / HCl / methanol / 24 h / 20 °C

3.1: DMAP; DCC / dimethylformamide / 12 h / 20 °C

4.1: triphenylphosphine; ADDP / tetrahydrofuran / 24 h / 20 °C

With dmap; sodium acetate; dicyclohexyl-carbodiimide; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: Substitution / 2.1: Substitution / 2.2: Hydrolysis / 3.1: Etherification / 4.1: Etherification;
DOI:10.1016/S0040-4020(00)00660-8