C₁₉H₃₁NO₃SSi

Base Information

• Chemical Name: C₁₉H₃₁NO₃SSi
• CAS No.: 1207463-12-4
• Molecular Formula: C₁₉H₃₁NO₃SSi
• Molecular Weight: 381.612
• Mol file: 1207463-12-4.mol

Synonyms:C₁₉H₃₁NO₃SSi

Chemical Property of C₁₉H₃₁NO₃SSi

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₉H₃₁NO₃SSi

There total 1 articles about C₁₉H₃₁NO₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

[3-(methoxymethoxy)-prop-1-enyl]trimethylsilane (929639-90-7) + (R,E)-2-methyl-N-(phenylmethylene)-2-propanesulfinamide (186249-76-3) → C19H31NO3SSi (1207463-12-4)

Guidance literature:

[3-(methoxymethoxy)-prop-1-enyl]trimethylsilane; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; hexane; cyclohexane; at -80 ℃; Inert atmosphere;

With zinc dibromide; In diethyl ether; hexane; cyclohexane; at -80 ℃; for 0.333333h; Inert atmosphere;

(R,E)-2-methyl-N-(phenylmethylene)-2-propanesulfinamide; In diethyl ether; hexane; cyclohexane; at -80 ℃; stereoselective reaction;

DOI:10.1055/s-0029-1218308

Reference yield:

C19H31NO3SSi (1207463-12-4) → C16H23NO3S

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.666667h;

DOI:10.1055/s-0029-1218308

upstream raw materials:

[3-(methoxymethoxy)-prop-1-enyl]trimethylsilane

(R,E)-2-methyl-N-(phenylmethylene)-2-propanesulfinamide