Technology Process of 2-amino-4-(2-methylpyridin-4-yl)phenol
There total 3 articles about 2-amino-4-(2-methylpyridin-4-yl)phenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
ethyl acetate;
under 517.162 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: caesium carbonate / N,N-dimethyl-formamide / 20 °C
2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / tris-(dibenzylideneacetone)dipalladium(0) / butan-1-ol / 100 °C
3: hydrogen / palladium 10% on activated carbon / ethyl acetate / 517.16 Torr
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; hydrogen; caesium carbonate;
tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon;
In
ethyl acetate; N,N-dimethyl-formamide; butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / tris-(dibenzylideneacetone)dipalladium(0) / butan-1-ol / 100 °C
2: hydrogen / palladium 10% on activated carbon / ethyl acetate / 517.16 Torr
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; hydrogen;
tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon;
In
ethyl acetate; butan-1-ol;
