4-ethynyl-4-hydroxycyclohexyl benzoate

Base Information

• Chemical Name: 4-ethynyl-4-hydroxycyclohexyl benzoate
• CAS No.: 874001-00-0
• Molecular Formula: C₁₅H₁₆O₃
• Molecular Weight: 244.29
• Mol file: 874001-00-0.mol

Synonyms:4-ethynyl-4-hydroxycyclohexyl benzoate

Chemical Property of 4-ethynyl-4-hydroxycyclohexyl benzoate

Chemical Property:

Purity/Quality:

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Technology Process of 4-ethynyl-4-hydroxycyclohexyl benzoate

There total 1 articles about 4-ethynyl-4-hydroxycyclohexyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4-ethynyl-4-hydroxycyclohexyl benzoate (874001-00-0)

Guidance literature:

With diethyl ether; ammonia; sodium acetylide;

DOI:10.1039/jr9490000615

Reference yield: 74.0%

4-ethynyl-4-hydroxycyclohexyl benzoate (874001-00-0) → 4-ethynylcyclohex-3-enyl benzoate (959864-86-9)

Guidance literature:

With pyridine; trichlorophosphate; at 90 ℃; for 1.5h;

DOI:10.1002/ejoc.200700367

Reference yield:

4-ethynyl-4-hydroxycyclohexyl benzoate (874001-00-0) → 4-Ethynyl-cyclohex-3-enol (33824-38-3)

Guidance literature:

Multistep reaction; (i) POCl₃, Py, (ii) aq. KOH, MeOH;

DOI:10.1039/j39710002960

Downstream raw materials:

4-Ethynyl-cyclohex-3-enol

4-ethynylcyclohex-3-enyl benzoate