N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine

Base Information

• Chemical Name: N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine
• CAS No.: 1643873-03-3
• Molecular Formula: C₃₇H₃₇NOS₂
• Molecular Weight: 575.839

Synonyms:N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine

Chemical Property of N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine

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Technology Process of N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine

There total 3 articles about N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

1,5-bis(2,5-dimethylthiophen-3-yl)-3-{4-[(4-methylphenyl)(4-methoxyphenyl)amino]phenyl}pentane-1,5-dione (1643872-97-2) → N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine (1643873-03-3)

Guidance literature:

With titanium tetrachloride; zinc; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Darkness;

DOI:10.1039/c4ra01601g

Reference yield:

3-Acetyl-2,5-dimethylthiophen (2530-10-1) → N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine (1643873-03-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.17 h / -25 °C / Inert atmosphere

1.2: 0.25 h / -25 °C / Inert atmosphere

2.1: zinc; titanium tetrachloride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere; Darkness

With titanium tetrachloride; zinc; lithium diisopropyl amide; In tetrahydrofuran; 2.1: |McMurry Reaction;

DOI:10.1039/c4ra01601g

Reference yield:

C37H37NOS2 → N-(4-methylphenyl)-N-(4-methoxyphenyl)-4-[3,4-bis(2,5-dimethyl-3-thienyl)-3-cyclopenten-1-yl]benzenamine (1643873-03-3)

Guidance literature:

In hexane; at 20 ℃; for 0.00833333h; Solvent; Quantum yield; Irradiation;

DOI:10.1039/c4ra01601g

upstream raw materials:

1,5-bis(2,5-dimethylthiophen-3-yl)-3-{4-[(4-methylphenyl)(4-methoxyphenyl)amino]phenyl}pentane-1,5-dione

3-Acetyl-2,5-dimethylthiophen

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