C₅₆H₇₅N₅O₁₁

Base Information

Chemical Name:C₅₆H₇₅N₅O₁₁
CAS No.:680620-93-3
Molecular Formula:C₅₆H₇₅N₅O₁₁
Molecular Weight:994.238
Hs Code.:

C<sub>56</sub>H<sub>75</sub>N<sub>5</sub>O<sub>11</sub>

Synonyms:C₅₆H₇₅N₅O₁₁

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Chemical Property of C₅₆H₇₅N₅O₁₁

Chemical Property:

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Technology Process of C₅₆H₇₅N₅O₁₁

There total 18 articles about C₅₆H₇₅N₅O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.4%

: 2-[2-(2-methoxyethoxy)ethoxy]ethyl 2-iodobenzoate

: 680620-91-1
C₄₂H₅₇N₅O₆

: 680620-93-3
C₅₆H₇₅N₅O₁₁

Guidance literature:: With copper(l) iodide; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; triethylamine; at 70 ℃; for 5h;
DOI:10.1021/ja039416d

Reference yield:

: 35998-96-0
methyl 5-amino-2-nitrobenzoate

: 680620-93-3
C₅₆H₇₅N₅O₁₁

Guidance literature:: Multi-step reaction with 11 steps

1.1: 78.3 percent / ICl; AcOH / 12 h

2.1: 93.8 percent / H₂SO₄ / CH₂Cl₂ / 1 h / 20 °C

3.1: 84.8 percent / AcOH / Fe / ethanol / 2 h / Heating

4.1: aq. NaNO₂; aq. HCl / acetonitrile / 0.5 h / 0 °C

4.2: 86.2 percent / K₂CO₃ / acetonitrile; H₂O / 0 - 20 °C

5.1: 93.8 percent / aq. NaOH / methanol / 0.5 h / Heating

6.1: 85.3 percent / DCC; DMAP / CH₂Cl₂ / 48 h / 20 °C

7.1: 93.8 percent / Pd(PPh₃)2Cl₂; CuI; Et₃N / 12 h / 40 °C

8.1: 90.2 percent / K₂CO₃ / methanol / 0.08 h / 20 °C

9.1: 88.9 percent / Pd(dba)2; CuI; PPh₃ / Et₃N / 24 h / 70 °C

10.1: 96.5 percent / K₂CO₃ / methanol; CH₂Cl₂ / 0.17 h / 20 °C

11.1: 69.4 percent / Pd(dba)2; CuI; PPh₃ / Et₃N / 5 h / 70 °C

With hydrogenchloride; dmap; bis-triphenylphosphine-palladium(II) chloride; sodium hydroxide; copper(l) iodide; sulfuric acid; Iodine monochloride; potassium carbonate; acetic acid; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium nitrite; iron; triethylamine; In methanol; ethanol; dichloromethane; acetonitrile; 7.1: Sonogashira coupling / 9.1: Sonogashira coupling / 11.1: Sonogashira coupling;
DOI:10.1021/ja039416d

Reference yield:

: 111-87-5
octanol

: 680620-93-3
C₅₆H₇₅N₅O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1: 85.3 percent / DCC; DMAP / CH₂Cl₂ / 48 h / 20 °C

2: 93.8 percent / Pd(PPh₃)2Cl₂; CuI; Et₃N / 12 h / 40 °C

3: 90.2 percent / K₂CO₃ / methanol / 0.08 h / 20 °C

4: 88.9 percent / Pd(dba)2; CuI; PPh₃ / Et₃N / 24 h / 70 °C

5: 96.5 percent / K₂CO₃ / methanol; CH₂Cl₂ / 0.17 h / 20 °C

6: 69.4 percent / Pd(dba)2; CuI; PPh₃ / Et₃N / 5 h / 70 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; triethylamine; In methanol; dichloromethane; 2: Sonogashira coupling / 4: Sonogashira coupling / 6: Sonogashira coupling;
DOI:10.1021/ja039416d