methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate

Base Information

Chemical Name:methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate
CAS No.:1448318-94-2
Molecular Formula:C₁₄H₁₇F₅O₄S
Molecular Weight:376.345
Hs Code.:

methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ<sup>6</sup>-sulphanyl)benzoate

Synonyms:methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate

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Chemical Property of methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate

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Technology Process of methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate

There total 2 articles about methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 833-96-5
3-(pentafluoro-λ⁶-sulphanyl)benzoic acid

: 1448318-94-2
methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; trifluoroacetic acid; N-Bromosuccinimide / 18 h / 50 °C

2.1: thionyl chloride / methanol / 4 h / Reflux

3.1: zinc; chloro-trimethyl-silane / tetrahydrofuran; diethyl ether / 1 h / Inert atmosphere; Reflux

3.2: 36 h / 20 - 60 °C / Inert atmosphere

With N-Bromosuccinimide; chloro-trimethyl-silane; thionyl chloride; sulfuric acid; trifluoroacetic acid; zinc; In tetrahydrofuran; methanol; diethyl ether;

Reference yield:

: 1180675-98-2
3-bromo-5-(pentafluoro-λ⁶-sulphanyl)benzoic acid

: 1448318-94-2
methyl 3-(2-tert-butoxy-2-oxoethyl)-5-(pentafluoro-λ⁶-sulphanyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / methanol / 4 h / Reflux

2.1: zinc; chloro-trimethyl-silane / tetrahydrofuran; diethyl ether / 1 h / Inert atmosphere; Reflux

2.2: 36 h / 20 - 60 °C / Inert atmosphere

With chloro-trimethyl-silane; thionyl chloride; zinc; In tetrahydrofuran; methanol; diethyl ether;