3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide

Base Information

Chemical Name:3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide
CAS No.:1607830-47-6
Molecular Formula:C₁₄H₁₀BrClN₄O
Molecular Weight:365.617
Hs Code.:

Synonyms:3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide

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Chemical Property of 3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide

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Technology Process of 3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide

There total 6 articles about 3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 932-96-7
N-methyl(p-chloroaniline)

: 1234015-04-3
3-bromoimidazo[1,2-a]pyrazine-6-carboxylic acid

: 1607830-47-6
3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide

Guidance literature:: 3-bromoimidazo[1,2-a]pyrazine-6-carboxylic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 0.5h;

N-methyl(p-chloroaniline); With triethylamine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 932-96-7
N-methyl(p-chloroaniline)

: 1607830-25-0
C₇H₃BrClN₃O

: 1607830-47-6
3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ml500244m

Reference yield:

: 588720-67-6
ethyl pyrrolo[1,2-a]pyrazine-3-carboxylate

: 1607830-47-6
3-bromo-N-(4-chlorophenyl)-N-methylimidazo[1,2-a]pyrazine-6-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dichloromethane / 3 h / 20 °C

2.1: sodium hydroxide / tetrahydrofuran; water / 1.5 h / 60 °C

3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

3.2: 3 h / 20 °C

With N-Bromosuccinimide; oxalyl dichloride; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;