(C₅H₄NC₅H₃NC₅H₄N)OsCl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)⁽¹⁺⁾*PF₆^(1-)=[Os(C₅H₄NC₅H₃NC₅H₄N)Cl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)][PF₆]

Base Information

• Chemical Name: (C₅H₄NC₅H₃NC₅H₄N)OsCl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)⁽¹⁺⁾*PF₆^(1-)=[Os(C₅H₄NC₅H₃NC₅H₄N)Cl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)][PF₆]
• CAS No.: 250655-38-0
• Molecular Formula: C₃₁H₂₇Cl₂N₄O₂Os*F₆P
• Molecular Weight: 893.651

Synonyms:(C₅H₄NC₅H₃NC₅H₄N)OsCl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)⁽¹⁺⁾*PF₆^(1-)=[Os(C₅H₄NC₅H₃NC₅H₄N)Cl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)][PF₆]

Chemical Property of (C₅H₄NC₅H₃NC₅H₄N)OsCl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)⁽¹⁺⁾*PF₆^(1-)=[Os(C₅H₄NC₅H₃NC₅H₄N)Cl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)][PF₆]

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Technology Process of (C₅H₄NC₅H₃NC₅H₄N)OsCl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)⁽¹⁺⁾*PF₆^(1-)=[Os(C₅H₄NC₅H₃NC₅H₄N)Cl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)][PF₆]

There total 2 articles about (C₅H₄NC₅H₃NC₅H₄N)OsCl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)⁽¹⁺⁾*PF₆^(1-)=[Os(C₅H₄NC₅H₃NC₅H₄N)Cl₂(CH₃OC₆H₄CHNCHC₆H₄OCH₃)][PF₆] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

cis-[Os(VI)(2,2':6',2''-terpyridine)(Cl)2(N)](PF6) (127571-48-6,159248-17-6) + 1,2-bis(4-methoxyphenyl)ethene (4705-34-4,15638-14-9,34480-01-8,112246-67-0,2510-75-0) → (C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNCHC6H4OCH3)(1+)*PF6(1-)=[Os(C5H4NC5H3NC5H4N)Cl2(CH3OC6H4CHNCHC6H4OCH3)][PF6] (250655-38-0)

Guidance literature:

In acetonitrile;

DOI:10.1021/ja992385v

Reference yield: 85.0%

cis-[Os(VI)(2,2':6',2''-terpyridine)(Cl)2(N)](PF6) (127571-48-6,159248-17-6) + 4,4'-dimethoxystilbene (4705-34-4) → cis-[(2,2':6',2''-terpyridine)OsCl2(1,2-η2-[4-MeOC6H4]CH=N=CH[4-MeOC6H4])]PF6 (250655-38-0)

Guidance literature:

In acetonitrile; soln. of Os-complex and ligand in MeCN was added into flask, heated at 65°C for 18 h under N2 or Ar; MeCN was evapd. on rotary evaporator, layered with ether, allowed to stand overnight at -20°C, filtered, washed with Et2O;

DOI:10.1021/om034404m

upstream raw materials:

cis-[Os(VI)(2,2':6',2''-terpyridine)(Cl)2(N)](PF₆)

1,2-bis(4-methoxyphenyl)ethene

4,4'-dimethoxystilbene

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