4'-acetamidophenyl 4-phenyl ether

Base Information

Chemical Name:4'-acetamidophenyl 4-phenyl ether
CAS No.:133041-70-0
Molecular Formula:C₁₈H₂₀Cl₂N₂O₂
Molecular Weight:367.275
Hs Code.:

4'-acetamidophenyl 4-<bis(2-chloroethyl)amino>phenyl ether

Synonyms:4'-acetamidophenyl 4-phenyl ether

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Chemical Property of 4'-acetamidophenyl 4-phenyl ether

Chemical Property:

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Technology Process of 4'-acetamidophenyl 4-phenyl ether

There total 5 articles about 4'-acetamidophenyl 4-phenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methanesulfonic acid 2-[[4-(4-acetylamino-phenoxy)-phenyl]-(2-methanesulfonyloxy-ethyl)-amino]-ethyl ester

: 133041-70-0
4'-acetamidophenyl 4-phenyl ether

Guidance literature:: With sodium chloride; In N,N-dimethyl-formamide; at 140 ℃; Yield given;
DOI:10.1021/jm00109a005

Reference yield:

: 103-90-2,8055-08-1
4-acetaminophenol

: 133041-70-0
4'-acetamidophenyl 4-phenyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaOH / 1.) EtOH, reflux, 30 min, 2.) reflux, 1 h

2: H₂ / 10percent Pd/C / methanol

3: 1 N aq. AcOH / 24 h

4: Et₃N

5: NaCl / dimethylformamide / 140 °C

With sodium hydroxide; hydrogen; acetic acid; triethylamine; sodium chloride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00109a005

Reference yield:

: 2687-40-3
4-nitrophenyl 4'-acetamidophenyl ether

: 133041-70-0
4'-acetamidophenyl 4-phenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / methanol

2: 1 N aq. AcOH / 24 h

3: Et₃N

4: NaCl / dimethylformamide / 140 °C

With hydrogen; acetic acid; triethylamine; sodium chloride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00109a005