[4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide

Base Information

Chemical Name:[4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide
CAS No.:337984-51-7
Molecular Formula:C₂₈H₂₆OS₃
Molecular Weight:474.712
Hs Code.:

Synonyms:[4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide

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Chemical Property of [4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide

Chemical Property:

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Technology Process of [4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide

There total 3 articles about [4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 103677-20-9
bis[4-(4-methylbenzylthio)phenyl]sulfide

: bis[4-(4-methylbenzylsulfinyl)phenyl]sulfide

: 337984-51-7
[4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -20 ℃;
DOI:10.1021/jo001645k

Reference yield:

: 19362-77-7
4,4'-dimercaptodiphenyl sulfide

: 337984-51-7
[4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / KOH / methanol / 0 °C

2: 34 percent / m-CPBA / CH₂Cl₂ / -20 °C

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1021/jo001645k

Reference yield:

: 104-82-5
4-Methylbenzyl chloride

: 337984-51-7
[4-(4-methylbenzylsulfinyl)phenyl]-[4'-(4'-methylbenzylthio)phenyl]sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / KOH / methanol / 0 °C

2: 34 percent / m-CPBA / CH₂Cl₂ / -20 °C

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1021/jo001645k