11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5,10-tetraene

Base Information

• Chemical Name: 11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5,10-tetraene
• CAS No.: 869592-97-2
• Molecular Formula: C₁₈H₁₅ClO₂
• Molecular Weight: 298.769

Synonyms:11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5,10-tetraene

Chemical Property of 11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5,10-tetraene

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Technology Process of 11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5,10-tetraene

There total 4 articles about 11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5,10-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,2-dihydrobenzocyclobuten-1-ol (35447-99-5) → 11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5,10-tetraene (869592-97-2)

Guidance literature:

1,2-dihydrobenzocyclobuten-1-ol; With n-butyllithium; In diethyl ether; at -78 - -25 ℃;

(CO)5W=C(OCH₃)CC(pClC₆H₅); In diethyl ether;

DOI:10.1002/anie.200501468

Reference yield: 86.0%

1,2-dihydrobenzocyclobuten-1-ol (35447-99-5) + C15H7ClO6W → 11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5,10-tetraene (869592-97-2)

Guidance literature:

1,2-dihydrobenzocyclobuten-1-ol; With n-butyllithium; In hexanes; diethyl ether; at -78 - -25 ℃; Inert atmosphere;

C₁₅H₇ClO₆W; In hexanes; diethyl ether; at -25 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201002092

Reference yield: 67.0%

1,2-dihydrobenzocyclobuten-1-ol (35447-99-5) → 11-(4-chlorophenyl)-9-methoxy-12-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5,10-tetraene (869592-97-2) + 6-(4-chlorophenyl)-8,9-dihydro-8-methoxy-5H-benzocyclohepten-5-one

Guidance literature:

1,2-dihydrobenzocyclobuten-1-ol; With n-butyllithium; In tetrahydrofuran; at -78 - -25 ℃;

(CO)5W=C(OCH₃)CC(pClC₆H₅); In tetrahydrofuran;

DOI:10.1002/anie.200501468

upstream raw materials:

1,2-dihydrobenzocyclobuten-1-ol

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