[3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide

Base Information

• Chemical Name: [3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide
• CAS No.: 1026700-75-3
• Molecular Formula: C₁₉H₁₉N₅O₃
• Molecular Weight: 365.392

Synonyms:[3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide

Chemical Property of [3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide

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Technology Process of [3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide

There total 1 articles about [3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

(3-benzoyl-4,5-dioxo-2-phenyl-pyrrolidin-1-yl)acetic acid ethyl ester (1026700-68-4) → (3-benzoyl-4,5-dioxo-2-phenyl-pyrrolidin-1-yl)acetic acid hydrazide (1026700-79-7) + [3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide (1026700-75-3)

Guidance literature:

With hydrazine hydrate; In ethanol; for 5h; Reflux;

DOI:10.1002/ardp.200700158

Reference yield: 88.0%

[3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide (1026700-75-3) + tetrachlorophthalic anhydride (117-08-8) → 2-{2,3-dioxo-5-phenyl-4-[phenyl-(4,5,6,7-tetrachloro-1,3-dioxo-1,3-dihydro-isoindol-2-ylimino)-methyl]pyrrolidin-1-yl}-N-(4,5,6,7-tetrachloro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-acetamide (1026700-86-6)

Guidance literature:

With acetic acid; at 80 ℃; for 6h;

DOI:10.1002/ardp.200700158

Reference yield: 86.0%

[3-(hydrazinophenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl]-acetic acid hydrazide (1026700-75-3) + 4-fluorobenzaldehyde (459-57-4) → (3-{[(4-fluorobenzylidene)hydrazono]-phenylmethyl}-4,5-dioxo-2-phenyl-pyrrolidin-1-yl)-acetic acid (4-fluorobenzylidine)-hydrazide (1026700-92-4)

Guidance literature:

In methanol; for 6h; Reflux;

DOI:10.1002/ardp.200700158

upstream raw materials:

(3-benzoyl-4,5-dioxo-2-phenyl-pyrrolidin-1-yl)acetic acid ethyl ester

Downstream raw materials:

N-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-{3-[(1,3-dioxo-1,3-dihydro-isoindol-2-ylimino)-phenylmethyl]-4,5-dioxo-2-phenyl-pyrrolidin-1-yl}-acetamide

(3-(ethylthiosemihydrazino-phenylmethyl)-4,5-dioxo-2-phenyl-pyrrolidin-1-yl)-acetic acid N'-thiopropionyl hydrazine

2-{2,3-dioxo-5-phenyl-4-[phenyl-(4,5,6,7-tetrachloro-1,3-dioxo-1,3-dihydro-isoindol-2-ylimino)-methyl]pyrrolidin-1-yl}-N-(4,5,6,7-tetrachloro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-acetamide

(3-{[(4-methylbenzylidene)hydrazono]-phenylmethyl}-4,5-dioxo-2-phenyl-pyrrolidin-1-yl)-acetic acid (4-methylbenzylidine)-hydrazide

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