tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile

Base Information

Chemical Name:tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile
CAS No.:777939-16-9
Molecular Formula:C₁₆H₁₈N₂OS
Molecular Weight:286.398
Hs Code.:

Synonyms:tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile

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Chemical Property of tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile

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Technology Process of tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile

There total 1 articles about tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 52989-47-6
2-amino-4,5-dihydro-5-methyl-3-thiophenecarbonitrile

: 122-57-6
1-Phenylbut-1-en-3-one

: 777939-16-9
tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile

Guidance literature:: With titanium tetrachloride; In chloroform; at 20 ℃; for 5h;
DOI:10.1002/jhet.5570410428

Reference yield: 73.0%

: 777939-16-9
tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile

: 1026855-51-5
2,3,3a,4-tetrahydro-2,6-dimethyl-4-phenylthieno[2,3-b]pyridine-3a-carbonitrile

Guidance literature:: With titanium tetrachloride; In chloroform; for 1h; Heating;
DOI:10.1002/jhet.5570410428

Reference yield:

: 777939-16-9
tetrahydro-2-imino-5-methyl-3-(3-oxo-1-phenylbutyl)-3-thiophenecarbonitrile

: 2,3-dihydro-2,6-dimethyl-4-phenylthieno[2,3-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / titanium(IV) chloride / CHCl₃ / 1 h / Heating

2: 84 percent / potassium tert-butoxide / 2-methyl-propan-2-ol / 1 h / Heating

With potassium tert-butylate; titanium tetrachloride; In chloroform; tert-butyl alcohol;
DOI:10.1002/jhet.5570410428