methyl (1α,2β,5β,6α)-7,7-diphenyl-3,8,9-triazatricyclo<4.3.0.0^2,5>non-8-ene-3-carboxylate

Base Information

• Chemical Name: methyl (1α,2β,5β,6α)-7,7-diphenyl-3,8,9-triazatricyclo<4.3.0.0^2,5>non-8-ene-3-carboxylate
• CAS No.: 105252-66-2
• Molecular Formula: C₂₀H₁₉N₃O₂
• Molecular Weight: 333.39

Synonyms:methyl (1α,2β,5β,6α)-7,7-diphenyl-3,8,9-triazatricyclo<4.3.0.0^2,5>non-8-ene-3-carboxylate

Chemical Property of methyl (1α,2β,5β,6α)-7,7-diphenyl-3,8,9-triazatricyclo<4.3.0.0^2,5>non-8-ene-3-carboxylate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Technology Process of methyl (1α,2β,5β,6α)-7,7-diphenyl-3,8,9-triazatricyclo<4.3.0.0^2,5>non-8-ene-3-carboxylate

There total 1 articles about methyl (1α,2β,5β,6α)-7,7-diphenyl-3,8,9-triazatricyclo<4.3.0.0^2,5>non-8-ene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-azabicyclo[2.2.0]hex-5-ene-2-carboxylate (33707-39-0) + diazodiphenylmethane (908093-98-1) → methyl (1α,2β,5β,6α)-9,9-diphenyl-3,7,8-triazatricyclo<4.3.0.02,5>non-7-ene-3-carboxylate (105252-65-1) + methyl (1α,2β,5β,6α)-7,7-diphenyl-3,8,9-triazatricyclo<4.3.0.02,5>non-8-ene-3-carboxylate (105252-66-2)

Guidance literature:

In toluene; at 80 ℃; for 11h; Yield given. Yields of byproduct given;

Reference yield: 88.0%

methyl (1α,2β,5β,6α)-7,7-diphenyl-3,8,9-triazatricyclo<4.3.0.02,5>non-8-ene-3-carboxylate (105252-66-2) → methyl (1α,2β,4β,5α)-3,3-diphenyl-6-azatricyclo<3.2.0.02,4>heptane-6-carboxylate (105252-70-8)

Guidance literature:

With benzophenone; In acetone; for 4h; Irradiation;

upstream raw materials:

methyl 2-azabicyclo[2.2.0]hex-5-ene-2-carboxylate

diazodiphenylmethane

Downstream raw materials:

methyl (1α,2β,4β,5α)-3,3-diphenyl-6-azatricyclo<3.2.0.0^2,4>heptane-6-carboxylate

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