3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone

Base Information

Chemical Name:3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone
CAS No.:110598-06-6
Molecular Formula:C₂₁H₃₀O₂
Molecular Weight:314.468
Hs Code.:

Synonyms:3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone

Chemical Property:

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Technology Process of 3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone

There total 6 articles about 3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.1%

: 110598-07-7
3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanol

: 110598-06-6
3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 3.25h; Ambient temperature;
DOI:10.1246/bcsj.59.3103

Reference yield:

: 14505-74-9,41721-03-3,59462-59-8,432-24-6
α-cyclocitral

: 110598-06-6
3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) hexane, benzene, 7-9 deg C, 30 min, 2.) hexane, benzene, 7-9 deg C, 1 h, room temperature, 3 h

2: 86.3 percent / ethanol / Ambient temperature

3: 4.530 g / 80percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / Ambient temperature

4: 60.5 percent / lithium diethylamide / hexane / 1.) -45 - -60 deg C, 30 min, 2.) room temperature, 30 min, 3.) reflux, 5 h

5: 89.1 percent / pyridinium chlorochromate / CH₂Cl₂ / 3.25 h / Ambient temperature

With lithium diethylamide; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; In ethanol; hexane; dichloromethane;
DOI:10.1246/bcsj.59.3103

Reference yield:

: 78478-90-7
3-(3-isopropyl-4-methoxyphenethyl)-2,4,4-trimethyl-1-cyclohexene

: 110598-06-6
3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 4.530 g / 80percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / Ambient temperature

2: 60.5 percent / lithium diethylamide / hexane / 1.) -45 - -60 deg C, 30 min, 2.) room temperature, 30 min, 3.) reflux, 5 h

3: 89.1 percent / pyridinium chlorochromate / CH₂Cl₂ / 3.25 h / Ambient temperature

With lithium diethylamide; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; In hexane; dichloromethane;
DOI:10.1246/bcsj.59.3103