Technology Process of 3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone
There total 6 articles about 3-(3-isopropyl-4-methoxyphenethyl)-4,4-dimethyl-2-methylenecyclohexanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
for 3.25h;
Ambient temperature;
DOI:10.1246/bcsj.59.3103
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) hexane, benzene, 7-9 deg C, 30 min, 2.) hexane, benzene, 7-9 deg C, 1 h, room temperature, 3 h
2: 86.3 percent / ethanol / Ambient temperature
3: 4.530 g / 80percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / Ambient temperature
4: 60.5 percent / lithium diethylamide / hexane / 1.) -45 - -60 deg C, 30 min, 2.) room temperature, 30 min, 3.) reflux, 5 h
5: 89.1 percent / pyridinium chlorochromate / CH2Cl2 / 3.25 h / Ambient temperature
With
lithium diethylamide; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate;
In
ethanol; hexane; dichloromethane;
DOI:10.1246/bcsj.59.3103
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 4.530 g / 80percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / Ambient temperature
2: 60.5 percent / lithium diethylamide / hexane / 1.) -45 - -60 deg C, 30 min, 2.) room temperature, 30 min, 3.) reflux, 5 h
3: 89.1 percent / pyridinium chlorochromate / CH2Cl2 / 3.25 h / Ambient temperature
With
lithium diethylamide; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate;
In
hexane; dichloromethane;
DOI:10.1246/bcsj.59.3103
