4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane)

Base Information

Chemical Name:4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane)
CAS No.:131846-17-8
Molecular Formula:C₂₅H₂₈O₄
Molecular Weight:392.495
Hs Code.:

Synonyms:4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane)

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Chemical Property of 4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane)

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane)

There total 1 articles about 4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 925211-06-9,925211-07-0
bicyclo(3.2.0)hept-2-en-6-one

: 17401-06-8
(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

: 131846-17-8
4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane)

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 8h; Heating;

Reference yield:

: 131846-17-8
4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane)

: 17401-06-8
(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromoacetamide / acetone; H₂O / Ambient temperature

2: 0.5 N H₂SO₄ / acetonitrile / 4 h / 70 °C

With sulfuric acid; N-bromoacetamide; In water; acetone; acetonitrile;

Reference yield:

: 131846-17-8
4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>hept-2-ene-6-spiro-2'-(1',3'-dioxolane)

: 131846-18-9,131900-35-1
1R,2S,3S,5R,4'S,5'S-2-bromo-3-hydroxy-4',5'-bis(benzyloxymethyl)bicyclo<3.2.0>heptane-6-spiro-2'-(1',3'-dioxolane)

Guidance literature:: Multi-step reaction with 3 steps

1: N-bromoacetamide / acetone; H₂O / Ambient temperature

2: 0.5 N H₂SO₄ / acetonitrile / 4 h / 70 °C

3: p-toluenesulfonic acid / toluene / 8 h / Heating

With sulfuric acid; toluene-4-sulfonic acid; N-bromoacetamide; In water; acetone; toluene; acetonitrile;