1-Mesityl-2-mesitylsulfonyl-acetylen

Base Information

Chemical Name:1-Mesityl-2-mesitylsulfonyl-acetylen
CAS No.:94757-02-5
Molecular Formula:C₂₀H₂₂O₂S
Molecular Weight:326.459
Hs Code.:

Synonyms:1-Mesityl-2-mesitylsulfonyl-acetylen

Suppliers and Price of 1-Mesityl-2-mesitylsulfonyl-acetylen

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Mesityl-2-mesitylsulfonyl-acetylen

Chemical Property:

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Technology Process of 1-Mesityl-2-mesitylsulfonyl-acetylen

There total 4 articles about 1-Mesityl-2-mesitylsulfonyl-acetylen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 94757-02-5
1-Mesityl-2-mesitylsulfonyl-acetylen

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / Heating

2: aq. H₂O₂, NaOH

3: (i) nBuLi, (ii) /BRN= 2058346/, (iii) aq. H₂O₂, Ac₂O, AcOH

With sodium hydroxide; lithium aluminium tetrahydride; dihydrogen peroxide; In diethyl ether;
DOI:10.1021/ja01483a031

Reference yield:

: 1541-10-2
mesitylthiol

: 94757-02-5
1-Mesityl-2-mesitylsulfonyl-acetylen

Guidance literature:: Multi-step reaction with 2 steps

1: aq. H₂O₂, NaOH

2: (i) nBuLi, (ii) /BRN= 2058346/, (iii) aq. H₂O₂, Ac₂O, AcOH

With sodium hydroxide; dihydrogen peroxide;
DOI:10.1021/ja01483a031

Reference yield:

: 5312-67-4
1-(1-chlorovinyl)-2',4',6'-trimethylbenzene

: 94757-02-5
1-Mesityl-2-mesitylsulfonyl-acetylen

Guidance literature:: Multi-step reaction with 2 steps

1: NaNH₂ / 160 °C

2: (i) nBuLi, (ii) /BRN= 2058346/, (iii) aq. H₂O₂, Ac₂O, AcOH

With sodium amide;
DOI:10.1021/ja01483a031