6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate

Base Information

Chemical Name:6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate
CAS No.:1380167-24-7
Molecular Formula:CH₄O₄S*C₁₄H₉Cl₃N₂OS
Molecular Weight:471.77
Hs Code.:

Synonyms:6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate

Chemical Property:

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Technology Process of 6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate

There total 6 articles about 6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-chloro-5-(2,3-dichlorophenoxy)-1H-benzimidazole-2-thiol: 68828-69-3
6-chloro-5-(2,3-dichlorophenoxy)-1H-benzimidazole-2-thiol

: 77-78-1
dimethyl sulfate

: 1380167-24-7
6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate

Guidance literature:: In methanol; at 40 - 65 ℃; for 6h; Industry scale;

Reference yield:

: 576-24-9
2,3-dichlorophenol

: 1380167-24-7
6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale

2.1: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale

3.1: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale

4.1: sodium hydroxide / methanol / 6 h / Reflux; Industry scale

4.2: 4 h / 60 - 90 °C / Industry scale

5.1: methanol / 6 h / 40 - 65 °C / Industry scale

With water; hydrogen; potassium carbonate; sodium hydroxide; Raney nickel; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 5462-30-6
N-(4,5-dichloro-2-nitrophenyl)acetamide

: 1380167-24-7
6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale

2.1: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale

3.1: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale

4.1: sodium hydroxide / methanol / 6 h / Reflux; Industry scale

4.2: 4 h / 60 - 90 °C / Industry scale

5.1: methanol / 6 h / 40 - 65 °C / Industry scale

With water; hydrogen; potassium carbonate; sodium hydroxide; Raney nickel; In methanol; N,N-dimethyl-formamide;