N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide

Base Information

• Chemical Name: N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide
• CAS No.: 946612-21-1
• Molecular Formula: C₃₆H₆Br₂F₁₀N₂O₄
• Molecular Weight: 880.247
• Mol file: 946612-21-1.mol

Synonyms:N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide

Chemical Property of N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide

There total 1 articles about N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

2,3,4,5,6-pentafluoroaniline (771-60-8) + 1,7-dibromoperylene-3,4,9,10-tetracarboxylic dianhydride (118129-60-5) → N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide (946612-21-1)

Guidance literature:

With acetic acid; In 1-methyl-pyrrolidin-2-one; at 160 ℃; for 28h;

Reference yield: 60.0%

bromopentafluorobenzene (344-04-7) + N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide (946612-21-1) → N,N'-1,7-tetrakis(2,3,4,5,6-pentafluorophenyl)perylene-3,4:9,10-bis(dicarboximide) (1202640-65-0)

Guidance literature:

With Cu-bronze; In N,N-dimethyl-formamide; at 140 ℃; for 16h;

DOI:10.1002/hlca.200900218

Reference yield: 45.0%

N,N'-bis(pentafluorophenyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxylic acid bisimide (946612-21-1) → N,N'-bis(pentafluorophenyl)-1,7-difluoroperylene-3,4:9,10-tetracarboxylic acid bisimide (946612-20-0)

Guidance literature:

With potassium fluoride; 18-crown-6 ether; In sulfolane; at 160 ℃; for 0.75h;

upstream raw materials:

2,3,4,5,6-pentafluoroaniline

1,7-dibromoperylene-3,4,9,10-tetracarboxylic dianhydride

Downstream raw materials:

N,N'-bis(pentafluorophenyl)-1,7-difluoroperylene-3,4:9,10-tetracarboxylic acid bisimide

N,N'-1,7-tetrakis(2,3,4,5,6-pentafluorophenyl)perylene-3,4:9,10-bis(dicarboximide)