ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate

Base Information

Chemical Name:ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate
CAS No.:220414-10-8
Molecular Formula:C₁₄H₁₃F₃N₂O₃
Molecular Weight:314.264
Hs Code.:

Synonyms:ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate

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Chemical Property of ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate

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Technology Process of ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate

There total 1 articles about ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 205485-25-2
2-methoxy-4-<3-trifluoromethyl-3H-diazirin-3-yl>benzaldehyde

: ethyl (Z)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate

: 220414-10-8
ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate

Guidance literature:: In toluene; at 20 ℃; for 2h;
DOI:10.3987/com-98-s25

Reference yield: 81.0%

: 220414-10-8
ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate

: ethyl 2,3-dihydroxy-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>propionate

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; butan-1-ol; at 20 ℃; for 48h;
DOI:10.3987/com-98-s25

Reference yield:

: 220414-10-8
ethyl (E)-3-<2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl>acrylate

: 205485-25-2
2-methoxy-4-<3-trifluoromethyl-3H-diazirin-3-yl>benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / OsO₄, 4-methylmorpholine N-oxide / H₂O; acetone; butan-1-ol / 48 h / 20 °C

2: 52 mg / sodium periodat / H₂O; acetone / 12 h / 20 °C

With sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; butan-1-ol;
DOI:10.3987/com-98-s25