1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone

Base Information

Chemical Name:1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone
CAS No.:886206-84-4
Molecular Formula:C₁₄H₁₀FNO₂S₂
Molecular Weight:307.369
Hs Code.:

Synonyms:1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone

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Chemical Property of 1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone

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Technology Process of 1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone

There total 7 articles about 1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 67219-33-4
2-phenylmethanesulfonyl-benzothiazole

: 886206-84-4
1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone

: 2-((difluoro(phenyl)methyl)sulfonyl)benzo[d]thiazole

Guidance literature:: 2-phenylmethanesulfonyl-benzothiazole; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; toluene; at -85 ℃; for 0.183333h;

With N-fluorobis(benzenesulfon)imide; In tetrahydrofuran; n-heptane; toluene; at -85 - 20 ℃;
DOI:10.1021/ol060002+

Reference yield: 90.0%

: 67219-33-4
2-phenylmethanesulfonyl-benzothiazole

: 886206-84-4
1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone

Guidance literature:: With N-fluorobis(benzenesulfon)imide; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; toluene; regiospecific reaction;
DOI:10.1021/acs.joc.5b02580

Reference yield:

: 19654-17-2
2-benzylthiobenzothiazole

: 886206-84-4
1,3-benzothiazol-2-yl (phenyl)fluoromethyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1.1: 94 percent / m-CPBA / CHCl₃ / -10 - 20 °C

2.1: LDA / toluene; tetrahydrofuran; heptane / 0.18 h / -85 °C

2.2: 90 percent / N-fluorobenzenesulfonimide / toluene; tetrahydrofuran; heptane / -85 - 20 °C

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; chloroform; toluene;
DOI:10.1021/ol060002+