2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole

Base Information

• Chemical Name: 2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole
• CAS No.: 1319211-88-5
• Molecular Formula: C₄₉H₄₇CuN₆O₂
• Molecular Weight: 815.497

Synonyms:2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole

Chemical Property of 2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole

There total 3 articles about 2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

[((NCCHCHC)3(CC6H4C(CH3)3)3(NCC(NO2)CHC))Cu] (1000044-87-0) → 2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole (1319211-88-5)

Guidance literature:

With 4-amino-1,2,4-triazole; sodium hydroxide; In ethanol; toluene; at 20 ℃; for 0.75h;

DOI:10.1021/ic2008073

Reference yield: 18.0%

4-amino-1,2,4-triazole (584-13-4) + [((NCCHCHC)3(CC6H4C(CH3)3)3(NCC(NO2)CHC))Cu] (1000044-87-0) → 2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole (1319211-88-5)

Guidance literature:

With NaOH; In ethanol; toluene; NaOH and triazole were added to soln. of Cu complex in toluene/EtOH (120/12); stirred at room temp. for 45 min; TLC monitoring; evapd. (vac.); dissolved in CHCl3; washed (aq. Na2S2O3);dried (Na2SO4); chromd. (silica gel, CHCl3); crystd. (CH2Cl2/MeOH); ele m. anal.;

DOI:10.1021/ic2008073

Reference yield:

H3(NCCHCHC)4(CC6H4C(CH3)3)3 → 2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole (1319211-88-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: NaOH / toluene; ethanol

With NaOH; In pyridine; ethanol; toluene;

DOI:10.1021/ic2008073

upstream raw materials:

[((NCCHCHC)3(CC₆H₄C(CH₃)3)3(NCC(NO₂)CHC))Cu]

4-amino-1,2,4-triazole

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1319211-88-5 2-amino-3-nitrotris( 5,10,15-tert-butylphenyl)corrole

Send

Send

Metric Ton KG G Pound L ML

Send

Send