ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate

Base Information

• Chemical Name: ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate
• CAS No.: 1393729-22-0
• Molecular Formula: C₂₆H₂₆N₂O₆
• Molecular Weight: 462.502

Synonyms:ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate

Chemical Property of ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate

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Technology Process of ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate

There total 2 articles about ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

ethyl 4-(3-oxobutanamido)benzoate (30764-23-9) → ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate (1393729-22-0)

Guidance literature:

With 2-methyltetrahydrofuran; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; copper(l) iodide; but-3-yn-2-ol; In toluene; at 110 ℃; for 5h;

DOI:10.1039/c5ra12115a

Reference yield: 78.0%

ethyl 3-(3-oxobutanamido)benzoate (1016675-89-0) → ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate (1393729-22-0)

Guidance literature:

With phosphorus pentoxide; zinc dibromide; In 1,4-dioxane; at 100 ℃; for 4h; Schlenk technique;

DOI:10.3762/bjoc.9.304

Reference yield: 94.0%

ethyl 4-(1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate (1393729-22-0) → ethyl 4-(5-bromo-1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate (1523153-41-4)

Guidance literature:

With pyridinium bromochromate; acetic acid; at 50 ℃; for 3h; regioselective reaction;

DOI:10.1080/00397911.2013.834363

upstream raw materials:

ethyl 4-(3-oxobutanamido)benzoate

ethyl 3-(3-oxobutanamido)benzoate

Downstream raw materials:

ethyl 4-(5-bromo-1-(4-(ethoxycarbonyl)phenyl)-2,6-dimethyl-4-oxo-1,4-dihydropyridine-3-carboxamido)benzoate

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