Technology Process of C32H26O12S2
There total 7 articles about C32H26O12S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
DOI:10.1021/ol990758r
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 98 percent / K2CO3 / CH2Cl2
2: 63 percent / NIS / CH2Cl2 / 20 °C
3: 72 percent / Cu-bronze / 210 - 220 °C
4: 55 percent / LDA / 0.08 h / -78 °C
5: 100 percent / CF3CO2H / H2O / Heating
6: 100 percent / MCPBA; K2CO3 / CH2Cl2
With
N-iodo-succinimide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; lithium diisopropyl amide;
In
dichloromethane; water;
3: Ullman coupling;
DOI:10.1021/ol990758r
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 72 percent / Cu-bronze / 210 - 220 °C
2: 55 percent / LDA / 0.08 h / -78 °C
3: 100 percent / CF3CO2H / H2O / Heating
4: 100 percent / MCPBA; K2CO3 / CH2Cl2
With
potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; lithium diisopropyl amide;
In
dichloromethane; water;
1: Ullman coupling;
DOI:10.1021/ol990758r