acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester

Base Information

Chemical Name:acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester
CAS No.:935676-91-8
Molecular Formula:C₁₈H₃₀O₄S₂
Molecular Weight:374.566
Hs Code.:

Synonyms:acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester

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Chemical Property of acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester

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Technology Process of acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester

There total 2 articles about acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52958-74-4
1-[(2-formylcyclohexyl)disulfanyl]cyclohexanecarbaldehyde

: 935676-91-8
acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaBH₄ / ethanol / 0.5 h / 0 °C

2: 91 percent / pyridine; DMAP / 48 h / 20 °C

With pyridine; dmap; sodium tetrahydroborate; In ethanol;
DOI:10.1021/ol070056z

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 935676-91-8
acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / S₂Cl₂ / CCl₄ / 18 h

2: 100 percent / NaBH₄ / ethanol / 0.5 h / 0 °C

3: 91 percent / pyridine; DMAP / 48 h / 20 °C

With pyridine; disulfur dichloride; dmap; sodium tetrahydroborate; In tetrachloromethane; ethanol;
DOI:10.1021/ol070056z

Reference yield: 97.0%

: 935676-91-8
acetic acid 1-(1-acetoxymethyl-cyclohexyldisulfanyl)-cyclohexylmethyl ester

: C₁₈H₃₀O₅S₂

Guidance literature:: With Oxone; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; Shi's ketone; edetate disodium; In acetonitrile; at 0 ℃; for 12h; pH=9.3;
DOI:10.1021/ol070056z