diisopropyl (E)-2-cyclohexylethenylphosphonate

Base Information

Chemical Name:diisopropyl (E)-2-cyclohexylethenylphosphonate
CAS No.:417712-02-8
Molecular Formula:C₁₄H₂₇O₃P
Molecular Weight:274.34
Hs Code.:

Synonyms:diisopropyl (E)-2-cyclohexylethenylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diisopropyl (E)-2-cyclohexylethenylphosphonate

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Technology Process of diisopropyl (E)-2-cyclohexylethenylphosphonate

There total 3 articles about diisopropyl (E)-2-cyclohexylethenylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1660-95-3
Tetraisopropyl methylenediphosphonate

: 2043-61-0
cyclohexanecarbaldehyde

: 417712-02-8
diisopropyl (E)-2-cyclohexylethenylphosphonate

Guidance literature:: Tetraisopropyl methylenediphosphonate; With sodium hydride; at 0 ℃; for 0.5h;

cyclohexanecarbaldehyde; at 0 ℃; for 0.333333h;
DOI:10.1016/S0040-4020(01)01089-4

Reference yield: 54.0%

: 1809-20-7
diisopropyl hydrogenphosphonate

: 60754-49-6
1,1-dibromo-2-cyclohexylethene

: 417712-02-8
diisopropyl (E)-2-cyclohexylethenylphosphonate

Guidance literature:: With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine; In toluene; at 120 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c0cc01617a

Reference yield:

: 1809-20-7
diisopropyl hydrogenphosphonate

: 60754-49-6
1,1-dibromo-2-cyclohexylethene

: (Z)-diisopropyl 2-cyclohexylvinylphosphonate

: 417712-02-8
diisopropyl (E)-2-cyclohexylethenylphosphonate

Guidance literature:: With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine; In toluene; at 120 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c0cc01617a