C₁₄H₂₁IO₄

Base Information

• Chemical Name: C₁₄H₂₁IO₄
• CAS No.: 1310492-05-7
• Molecular Formula: C₁₄H₂₁IO₄
• Molecular Weight: 380.223
• Mol file: 1310492-05-7.mol

Synonyms:C₁₄H₂₁IO₄

Chemical Property of C₁₄H₂₁IO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₁IO₄

There total 7 articles about C₁₄H₂₁IO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C14H21BrO4 (1310492-03-5) → C14H21IO4 (1310492-05-7)

Guidance literature:

With sodium iodide; In acetone; at 60 ℃;

DOI:10.1055/s-0030-1259918

Reference yield:

C10H17BrO2 (1310492-02-4) → C14H21IO4 (1310492-05-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,2,6,6-tetramethylpiperidinyl-lithium / tetrahydrofuran / -78 °C

2: sodium iodide / acetone / 60 °C

With 2,2,6,6-tetramethylpiperidinyl-lithium; sodium iodide; In tetrahydrofuran; acetone; 1: Michael condensation / 1: Claisen condensation;

DOI:10.1055/s-0030-1259918

Reference yield:

C20H29NO4 (1310492-00-2) → C14H21IO4 (1310492-05-7)

Guidance literature:

Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / -30 °C

2: tetrafluoroboric acid diethyl ether / dichloromethane / 20 °C

3: hydrogen bromide; acetic acid / 75 °C

4: 2,2,6,6-tetramethylpiperidinyl-lithium / tetrahydrofuran / -78 °C

5: sodium iodide / acetone / 60 °C

With tetrafluoroboric acid diethyl ether; lithium aluminium tetrahydride; 2,2,6,6-tetramethylpiperidinyl-lithium; hydrogen bromide; acetic acid; sodium iodide; In tetrahydrofuran; dichloromethane; acetone; 4: Michael condensation / 4: Claisen condensation;

DOI:10.1055/s-0030-1259918

upstream raw materials:

C₂₀H₂₉NO₄

C₁₉H₂₉NO₃

C₁₀H₁₇BrO₂

C₁₄H₂₁BrO₄