(3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne

Base Information

Chemical Name:(3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne
CAS No.:1253378-81-2
Molecular Formula:C₃₃H₅₂O₄Si₂
Molecular Weight:568.944
Hs Code.:

Synonyms:(3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne

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Technology Process of (3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne

There total 1 articles about (3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1253378-80-1
(3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-1-hexyn-3,4-diol

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 1253378-81-2
(3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1002/chem.201000795

Reference yield: 50.0%

: 1253378-81-2
(3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne

: 1253378-82-3
(3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3-triethylsiloxy-1-hexyn-4-ol

Guidance literature:: (3R,4R)-6-(4-methoxyphenylmethyloxy)-3-methyl-1-phenyl-3,4-ditriethylsiloxy-1-hexyne; With pyridinium p-toluenesulfonate; In diethyl ether; at 20 ℃; for 1h;

With water; sodium hydrogencarbonate; In diethyl ether; at 20 ℃; chemospecific reaction;
DOI:10.1002/chem.201000795