8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene

Base Information

• Chemical Name: 8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene
• CAS No.: 109888-82-6
• Molecular Formula: C₂₇H₃₃N₃O₅S
• Molecular Weight: 511.642

Synonyms:8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene

Chemical Property of 8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene

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Technology Process of 8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene

There total 2 articles about 8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

8-(Toluene-4-sulfonyl)-7,8,9,10-tetrahydro-6H,16H,22H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene-17,21-dione (120340-68-3) → 8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene (109888-82-6)

Guidance literature:

With diborane; In tetrahydrofuran;

DOI:10.1007/BF00479353

Reference yield:

1,5-bis(2-aminophenoxy)-3-(4-toluenesulfonyl)-3-azapentane (54533-68-5) → 8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene (109888-82-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / pyridine / dioxane; benzene / 6 h / 75 °C

2: 86 percent / B₂H₆ / tetrahydrofuran

With pyridine; diborane; In tetrahydrofuran; 1,4-dioxane; benzene;

DOI:10.1007/BF00479353

Reference yield: 59.0%

8-(Toluene-4-sulfonyl)-7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene (109888-82-6) → 7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene (54533-75-4)

Guidance literature:

With hydrogen bromide; phenol; In acetic acid; for 6h; Heating;

DOI:10.1007/BF00479353

upstream raw materials:

8-(Toluene-4-sulfonyl)-7,8,9,10-tetrahydro-6H,16H,22H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene-17,21-dione

1,5-bis(2-aminophenoxy)-3-(4-toluenesulfonyl)-3-azapentane

Downstream raw materials:

7,8,9,10,17,18,21,22-octahydro-6H,16H,20H-5,11,19-trioxa-8,16,22-triaza-dibenzo[a,j]cyclooctadecene

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