4,9-bis(4-(diphenylamino)phenyl)-2,7-bis(2-ethylhexyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

Base Information

Chemical Name:4,9-bis(4-(diphenylamino)phenyl)-2,7-bis(2-ethylhexyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone
CAS No.:1257127-92-6
Molecular Formula:C₆₆H₆₄N₄O₄
Molecular Weight:977.259
Hs Code.:

Synonyms:4,9-bis(4-(diphenylamino)phenyl)-2,7-bis(2-ethylhexyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

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Chemical Property of 4,9-bis(4-(diphenylamino)phenyl)-2,7-bis(2-ethylhexyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

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Technology Process of 4,9-bis(4-(diphenylamino)phenyl)-2,7-bis(2-ethylhexyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

There total 2 articles about 4,9-bis(4-(diphenylamino)phenyl)-2,7-bis(2-ethylhexyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1088205-02-0
N,N’-bis(2-ethylhexyl)-2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid bisimide

: diphenyl-(4-tributylstannanyl-phenyl)-amine

: 1257127-92-6
4,9-bis(4-(diphenylamino)phenyl)-2,7-bis(2-ethylhexyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2010.09.041

Reference yield: 40.0%

: 267221-88-5
4-(diphenylamino)phenylboronic pinacol ester

: 1088205-02-0
N,N’-bis(2-ethylhexyl)-2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid bisimide

: 1257127-92-6
4,9-bis(4-(diphenylamino)phenyl)-2,7-bis(2-ethylhexyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336; potassium carbonate; In water; toluene; at 120 ℃; for 24h; Concentration; Temperature; Inert atmosphere;