(4-cyclopropanesulfonyl-phenyl) diazo acetic acid ethyl ester

Base Information

Chemical Name:(4-cyclopropanesulfonyl-phenyl) diazo acetic acid ethyl ester
CAS No.:1234703-41-3
Molecular Formula:C₁₃H₁₄N₂O₄S
Molecular Weight:294.331
Hs Code.:
Mol file:1234703-41-3.mol

Synonyms:(4-cyclopropanesulfonyl-phenyl)-diazo-acetic acid ethyl ester

Suppliers and Price of (4-cyclopropanesulfonyl-phenyl) diazo acetic acid ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of (4-cyclopropanesulfonyl-phenyl) diazo acetic acid ethyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of (4-cyclopropanesulfonyl-phenyl) diazo acetic acid ethyl ester

There total 4 articles about (4-cyclopropanesulfonyl-phenyl) diazo acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313812-55-3
(4-cyclopropylsulfonyl)phenyl-oxo-acetic acid ethyl ester p-toluene sulfonyl hydrazone

: 1234703-41-3
(4-cyclopropanesulfonyl-phenyl)-diazo-acetic acid ethyl ester

Guidance literature:: With triethylamine; In ethyl acetate;

Reference yield:

: 14633-54-6
cyclopropylphenylsulfide

: 1234703-41-3
(4-cyclopropanesulfonyl-phenyl)-diazo-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

1.2: 2 h / 25 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 - 25 °C

3.1: toluene / 16 h / Reflux

4.1: triethylamine / dichloromethane / 1 h / 25 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; aluminum (III) chloride; In dichloromethane; toluene;

Reference yield:

: 876063-40-0
(4-cyclopropylsulfonylphenyl)-2-oxo-acetic acid ethyl ester

: 1234703-41-3
(4-cyclopropanesulfonyl-phenyl)-diazo-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 16 h / Reflux; a Dean-Stark apparatus

2: triethylamine / dichloromethane / 1 h / 25 °C

With triethylamine; In dichloromethane; toluene;