C₈H₁₃BrO₄

Base Information

Chemical Name:C₈H₁₃BrO₄
CAS No.:1514823-92-7
Molecular Formula:C₈H₁₃BrO₄
Molecular Weight:253.093
Hs Code.:

C<sub>8</sub>H<sub>13</sub>BrO<sub>4</sub>

Synonyms:C₈H₁₃BrO₄

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Chemical Property of C₈H₁₃BrO₄

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Technology Process of C₈H₁₃BrO₄

There total 5 articles about C₈H₁₃BrO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1514823-90-5
C₁₁H₁₇BrO₄

: 1514823-92-7
C₈H₁₃BrO₄

Guidance literature:: With water; acetic acid; at 70 ℃; for 14h;
DOI:10.1021/ol403220t

Reference yield:

: 183674-17-1
(1R,2S,5S,6R)-3,6-dibromo-1,2-O-isopropylidenecyclohex-3-ene-1,2,5-triol

: 1514823-92-7
C₈H₁₃BrO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 14 h / 18 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

2.2: 4 h / 18 °C

3.1: acetic acid; water / 14 h / 70 °C

With water; sodium hydride; acetic acid; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1021/ol403220t

Reference yield:

: 67451-62-1,82683-92-9,132958-32-8,130792-45-9
cis-(1S,2S)-1,2-dihydroxy-3-bromocyclohexa-3,5-diene

: 1514823-92-7
C₈H₁₃BrO₄

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide / water; tetrahydrofuran / 3 h / 18 °C

2: toluene-4-sulfonic acid / 2 h / 18 °C

3: methanol / 6 h / 0 - 18 °C

4: sodium hydride / tetrahydrofuran / 4.5 h / 0 - 18 °C

5: acetic acid / water / 14 h / 70 °C

With N-Bromosuccinimide; sodium hydride; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; methanol; water;
DOI:10.1021/jo500210k