(2Z,2′Z)-2,2′-(4-phenyl-1,2,4-dithiazolidine-3,5-diylidene)bis(1-phenylethanone)

Base Information

• Chemical Name: (2Z,2′Z)-2,2′-(4-phenyl-1,2,4-dithiazolidine-3,5-diylidene)bis(1-phenylethanone)
• CAS No.: 72891-73-7
• Molecular Formula: C₂₄H₁₇NO₂S₂
• Molecular Weight: 415.536
• Mol file: 72891-73-7.mol

Synonyms:(2Z,2′Z)-2,2′-(4-phenyl-1,2,4-dithiazolidine-3,5-diylidene)bis(1-phenylethanone)

Chemical Property of (2Z,2′Z)-2,2′-(4-phenyl-1,2,4-dithiazolidine-3,5-diylidene)bis(1-phenylethanone)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (2Z,2′Z)-2,2′-(4-phenyl-1,2,4-dithiazolidine-3,5-diylidene)bis(1-phenylethanone)

There total 2 articles about (2Z,2′Z)-2,2′-(4-phenyl-1,2,4-dithiazolidine-3,5-diylidene)bis(1-phenylethanone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N-phenyl-3-oxo-3-phenylpropanethioamide (13196-40-2) → (2Z,2′Z)-2,2′-(4-phenyl-1,2,4-dithiazolidine-3,5-diylidene)bis(1-phenylethanone) (72891-73-7)

Guidance literature:

With eosin; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Reagent/catalyst; Solvent; Irradiation;

DOI:10.1021/acs.joc.9b00406

Reference yield:

N-phenyl-3-oxo-3-phenylpropanethioamide (13196-40-2) → 1,1'-diphenyl-2,2'-((3E,5Z)-4-phenyl-[1,2,4]dithiazolidine-3,5-diylidene)-bis-ethanone (72891-72-6) + (2Z,2′Z)-2,2′-(4-phenyl-1,2,4-dithiazolidine-3,5-diylidene)bis(1-phenylethanone) (72891-73-7)

Guidance literature:

With bromine; In chloroform; at -10 ℃; for 0.583333h;

DOI:10.1007/BF00471427

upstream raw materials:

N-phenyl-3-oxo-3-phenylpropanethioamide