N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide

Base Information

Chemical Name:N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide
CAS No.:13202-03-4
Molecular Formula:C₂₆H₂₄N₆O₂
Molecular Weight:452.516
Hs Code.:

Synonyms:N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide

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Chemical Property of N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide

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Technology Process of N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide

There total 5 articles about N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143330-23-8
4-[(4-cyanobenzoyl)amino]benzoic acid

: 13202-03-4
N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide; thionyl chloride / dichloromethane / 24 h / 20 °C

2: triethylamine; dmap / N,N-dimethyl acetamide / 24 h / 20 °C

3: sodium hydrogen sulfide / N,N-dimethyl acetamide / 2 h / 120 °C

With dmap; sodium hydrogen sulfide; thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2013.12.064

Reference yield:

: 6068-72-0
4-cyanobenzoyl chlorIde

: 13202-03-4
N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: dmap / N,N-dimethyl acetamide / 24 h / 20 °C / Inert atmosphere

2: N,N-dimethyl-formamide; thionyl chloride / dichloromethane / 24 h / 20 °C

3: triethylamine; dmap / N,N-dimethyl acetamide / 24 h / 20 °C

4: sodium hydrogen sulfide / N,N-dimethyl acetamide / 2 h / 120 °C

With dmap; sodium hydrogen sulfide; thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2013.12.064

Reference yield:

: 1158816-11-5
4-(4-cyanobenzoylamino)benzoyl chloride

: 13202-03-4
N-[4-(4,5-dihydro-1H-imidazol-2-yl)phenyl]-4-[[4-(4,5-dihydro-1H-imidazol-2-yl)benzoyl]amino]benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; dmap / N,N-dimethyl acetamide / 24 h / 20 °C

2: sodium hydrogen sulfide / N,N-dimethyl acetamide / 2 h / 120 °C

With dmap; sodium hydrogen sulfide; triethylamine; In N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2013.12.064