C₂₂H₂₈O₅S

Base Information

• Chemical Name: C₂₂H₂₈O₅S
• CAS No.: 1352496-99-1
• Molecular Formula: C₂₂H₂₈O₅S
• Molecular Weight: 404.527
• Mol file: 1352496-99-1.mol

Synonyms:C₂₂H₂₈O₅S

Chemical Property of C₂₂H₂₈O₅S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₈O₅S

There total 6 articles about C₂₂H₂₈O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C29H31NO8S (1352496-98-0) → C22H28O5S (1352496-99-1)

Guidance literature:

With methanol; potassium carbonate; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2011.09.011

Reference yield:

C22H26O5S (1352496-70-8) → C22H28O5S (1352496-99-1)

Guidance literature:

Multi-step reaction with 3 steps

1: samarium diiodide / tetrahydrofuran; methanol / 0 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 20 °C / Inert atmosphere

3: methanol; potassium carbonate / 20 °C / Inert atmosphere

With methanol; samarium diiodide; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; toluene; 2: Mitsunobu reaction;

DOI:10.1016/j.tet.2011.09.011

Reference yield:

C22H28O5S (1352496-72-0) → C22H28O5S (1352496-99-1)

Guidance literature:

Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 20 °C / Inert atmosphere

2: methanol; potassium carbonate / 20 °C / Inert atmosphere

With methanol; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In toluene; 1: Mitsunobu reaction;

DOI:10.1016/j.tet.2011.09.011

upstream raw materials:

C₂₂H₂₆O₅S

C₂₂H₂₈O₅S

C₂₉H₃₁NO₈S

C₁₆H₂₄O₃S₂

Downstream raw materials:

C₂₂H₃₆O₅Si

C₃₀H₅₀O₅Si

C₃₀H₅₀O₅Si

C₃₆H₆₄O₅Si₂