(R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol

Base Information

• Chemical Name: (R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol
• CAS No.: 848830-54-6
• Molecular Formula: C₃₆H₃₈O₇
• Molecular Weight: 582.694

Synonyms:(R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol

Chemical Property of (R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of (R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol

There total 1 articles about (R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(1-methylethyl)phenol (88-69-7) → (R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol (848830-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 0.58 h

1.2: 85 percent / tetrahydrofuran / 0 - 20 °C

2.1: n-BuLi; TMEDA / hexane; tetrahydrofuran / 1 h / -78 - 0 °C

2.2: 85 percent / hexane; tetrahydrofuran / -78 - 0 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; In tetrahydrofuran; hexane;

DOI:10.1021/ja053524d

Reference yield: 85.0%

(R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol (848830-54-6) → 3-[hydroxy-(2-hydroxy-3-isopropyl-phenyl)-methyl]-[1,1']binaphthalenyl-2,2'-diol

Guidance literature:

With hydrogenchloride; In methanol; dichloromethane; at 0 ℃; for 1h;

DOI:10.1021/ja053524d

Reference yield:

(R)-[2,2'-bis(methoxymethyloxy)-1,1'-binaphthyl-3-yl]-(3-isopropyl-2-methoxymethyloxyphenyl)methanol (848830-54-6) → (R)-3-[(R)-(2-hydroxy-3-isopropylphenyl)-methoxymethyl]-1,1'-binaphthalene-2,2'-diol

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.75 h / 20 °C

1.2: 88 percent / dimethylformamide / 0 - 20 °C

2.1: 31 percent / HCl / methanol; CH₂Cl₂ / 2 h / 0 °C

With hydrogenchloride; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja053524d

upstream raw materials:

2-(1-methylethyl)phenol

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