(R)-1-diphenylphosphinyl-2-vinylferrocene

Base Information

Chemical Name:(R)-1-diphenylphosphinyl-2-vinylferrocene
CAS No.:55650-56-1
Molecular Formula:C₂₄H₂₁FeOP
Molecular Weight:412.251
Hs Code.:

Synonyms:(R)-1-diphenylphosphinyl-2-vinylferrocene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-diphenylphosphinyl-2-vinylferrocene

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Technology Process of (R)-1-diphenylphosphinyl-2-vinylferrocene

There total 1 articles about (R)-1-diphenylphosphinyl-2-vinylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: (S)-N,N-dimethyl-1-[(R)-2-(diphenylphosphinyl)ferrocenyl]ethylamine

: 55650-56-1
(R)-1-diphenylphosphinyl-2-vinylferrocene

Guidance literature:: With methyl iodide; In acetone; addition of MeI at room temperature to soln. of complex, refluxed for 15 min, N2 atm.; concn. in vac., dilution with benzene, washing with 8.5% phosphoric acid and 10% NaOH, drying over Na2SO4, evapn., chromy. (silica gel, benzene/ethyl acetate 3/1);
DOI:10.1246/bcsj.53.1138

Reference yield:

: 55650-56-1
(R)-1-diphenylphosphinyl-2-vinylferrocene

: 74286-13-8
(R)-1-diphenylphosphinyl-2-ethylferrocene

Guidance literature:: With hydrogen; Wilkinson's catalyst; In benzene; hydrogenated at 130 kg/cm*2; chromy. (alumina, benzene/ethyl acetate 2/1); elem. anal.;
DOI:10.1246/bcsj.53.1138