6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.0^2,4>hexane

Base Information

• Chemical Name: 6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.0^2,4>hexane
• CAS No.: 64724-57-8
• Molecular Formula: C₁₄H₁₁F₁₂NS
• Molecular Weight: 453.295

Synonyms:6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.0^2,4>hexane

Chemical Property of 6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.0^2,4>hexane

Chemical Property:

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Technology Process of 6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.0^2,4>hexane

There total 1 articles about 6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.0^2,4>hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.9%

8-cyclohexyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.02,4]oct-6-ene (64724-55-6) → 6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.02,4>hexane (64724-57-8)

Guidance literature:

In pentane; for 6.5h; Irradiation; sealed tube (under vacuum);

DOI:10.1021/jo01303a010

Reference yield:

6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.02,4>hexane (64724-57-8) → N-cyclohexyl (Dewar pyrrole) (64724-58-9)

Guidance literature:

With triphenylphosphine; In pentane; Yield given;

DOI:10.1021/jo01303a010

Reference yield:

6-cyclohexyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.02,4>hexane (64724-57-8) → 4-cyclohexyl-2,3,5,6-tetrakis(trifluoromethyl)-4-aza-10-oxatetracyclo<5.2.1.02,6.03,5>dec-8-ene (64724-59-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triphenylphosphine / pentane

2: CHCl₃ / 0.5 h / Ambient temperature

With triphenylphosphine; In chloroform; pentane;

DOI:10.1021/jo01303a010

upstream raw materials:

8-cyclohexyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene

Downstream raw materials:

N-cyclohexyl (Dewar pyrrole)

4-cyclohexyl-2,3,5,6-tetrakis(trifluoromethyl)-4-aza-10-oxatetracyclo<5.2.1.0^2,6.0^3,5>dec-8-ene

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