N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester

Base Information

Chemical Name:N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester
CAS No.:118597-41-4
Molecular Formula:C₂₆H₂₈N₄O₇S
Molecular Weight:540.597
Hs Code.:

Synonyms:N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester

Chemical Property:

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Technology Process of N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester

There total 1 articles about N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63-74-1
sulfanilamide

: 89625-84-3
N-carboxybenzoxy-L-alanyl-D,L-2-acetoxyglycine benzyl ester

: 118597-41-4
N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00123a034

Reference yield: 82.0%

: 118597-41-4
N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester

: 118597-50-5
L-Alanyl-D,L-2-<<4-(aminosulfonyl)phenyl>amino>glycine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; under 2585.7 Torr;
DOI:10.1021/jm00123a034

Reference yield:

: 118597-41-4
N-Carbobenzoxy-L-alanyl-D,L-<<4-(aminosulfonyl)phenyl>amino>glycine benzyl ester

: 118597-54-9
N-Carbobenzoxy-L-alanyl-L-alanyl-D,L-2-<<4-(aminosulfonyl)phenyl>amino>glycine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / H₂ / 10percent Pd-C / methanol / 3 h / 2585.7 Torr

2: 43 percent / Et₃N, 4 Angstroem molecular sieves / dimethylformamide / 1) 5 deg C, 3 h, 2) r.t., overnight

With 4 A molecular sieve; hydrogen; triethylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00123a034