tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium

Base Information

Chemical Name:tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium
CAS No.:83399-44-4
Molecular Formula:C₂₂H₃₇N₄ReS₆
Molecular Weight:736.166
Hs Code.:

Synonyms:tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium

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Chemical Property of tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium

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Technology Process of tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium

There total 5 articles about tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 83399-40-0
chlorobis(diethyldithiocarbamato)(p-tolylnitrene)rhenium

: 83399-44-4
tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium

Guidance literature:: With trimethylsilyl diethyldithiocarbamate; In benzene; under N2, to refluxing soln. of Re-complex in dry benzene added trimethylsilyl diethyldithiocarbamate, refluxed for 5 min, cooled; vol. reduced, dry acetone added, filtered, washed with acetone and hexane; elem. anal.;

Reference yield: 79.0%

: Re(PPh₃)2(NC₆H₄Me-p)Cl₃

: 83399-44-4
tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium

Guidance literature:: With trimethylsilyl ethyldithiocarbamate; In benzene; under N2, to soln. of Re-complex in benzene added trimethylsilyl diethyldithiocarbamate, refluxed for 10 min; vol. reduced, dry acetone added, filtered, washed with acetone and hexane, dried; elem. anal.;

Reference yield: 78.0%

: Re(PPh₃)2(NC₆H₄Me-p)Cl₃

: 113278-24-3
diethylcarbamoyldithioato-SS'-thallium

: 83399-44-4
tris(diethyldithiocarbamato)(p-tolylnitrene)rhenium

Guidance literature:: In benzene; byproducts: TlCl; under N2, Re-complex and thallium diethyldithiocarbamate (molar ratio 1:3) added to benzene, refluxed for 10 min, cooled; filtered, vol. reduced, dry acetone added, filtered, washed with acetone and hexane, dried; elem. anal.;