(3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one

Base Information

Chemical Name:(3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one
CAS No.:82706-59-0
Molecular Formula:C₁₆H₁₈INO₃
Molecular Weight:399.228
Hs Code.:

Synonyms:(3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one

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Chemical Property of (3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one

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Technology Process of (3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one

There total 3 articles about (3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 82706-71-6
2-Benzoylamino-2-cyclohex-2-enyl-propionic acid

: 82706-59-0
(3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one

Guidance literature:: With iodine; sodium hydrogencarbonate; potassium iodide; In diethyl ether; at 21 ℃; for 0.5h;
DOI:10.1021/jo00141a024

Reference yield:

: 82706-63-6
4-Cyclohex-2-enyl-4-methyl-2-phenyl-4H-oxazol-5-one

: 82706-59-0
(3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / NaOH / methanol / 1.5 h / 55 °C

2: 22 percent / I₂, KI, NaHCO₃ / diethyl ether / 0.5 h / 21 °C

With sodium hydroxide; iodine; sodium hydrogencarbonate; potassium iodide; In methanol; diethyl ether;
DOI:10.1021/jo00141a024

Reference yield:

: 82706-54-5
2-Benzoylamino-propionic acid cyclohex-2-enyl ester

: 82706-59-0
(3RS,3aRS,7SR,7aSR)-3-(benzoylamino)hexahydro-7-iodo-3-methylbenzofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / (C₆H₅)3P, (C₂H₅)3N / CCl₄; acetonitrile

2: 43 percent / NaOH / methanol / 1.5 h / 55 °C

3: 22 percent / I₂, KI, NaHCO₃ / diethyl ether / 0.5 h / 21 °C

With sodium hydroxide; iodine; sodium hydrogencarbonate; triethylamine; triphenylphosphine; potassium iodide; In methanol; tetrachloromethane; diethyl ether; acetonitrile;
DOI:10.1021/jo00141a024