Fmoc(BocApi)2OBn

Base Information

Chemical Name:Fmoc(BocApi)2OBn
CAS No.:1246024-65-6
Molecular Formula:C₄₄H₅₄N₄O₉
Molecular Weight:782.934
Hs Code.:

Synonyms:Fmoc(BocApi)2OBn

Suppliers and Price of Fmoc(BocApi)2OBn

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Fmoc(BocApi)2OBn

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Fmoc(BocApi)2OBn

There total 1 articles about Fmoc(BocApi)2OBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1246024-64-5
H(BocApi)OBn

: 183673-66-7
N-Fmoc-amino-(4-N-Boc-piperidinyl)carboxylic acid

: 1246024-65-6
Fmoc(BocApi)2OBn

Guidance literature:: N-Fmoc-amino-(4-N-Boc-piperidinyl)carboxylic acid; With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.5h;

H(BocApi)OBn; With 2,4,6-trimethyl-pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ja106118w

Reference yield: 97.0%

: 1246024-65-6
Fmoc(BocApi)2OBn

: 1246024-67-8
H(BocApi)2OBn

Guidance literature:: With diethylamine; In tetrahydrofuran;
DOI:10.1021/ja106118w

Reference yield:

: 1246024-65-6
Fmoc(BocApi)2OBn

: 1246024-70-3
H(BocApi)4OBn

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium on activated carbon / methanol; tetrahydrofuran / 760.05 Torr

2: 1-hydroxy-7-aza-benzotriazole / dichloromethane

3: diethylamine / tetrahydrofuran

With 1-hydroxy-7-aza-benzotriazole; palladium on activated carbon; hydrogen; diethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.201605460