C₂₇H₃₃Cl₂N₇O₅S

Base Information

Chemical Name:C₂₇H₃₃Cl₂N₇O₅S
CAS No.:1353629-09-0
Molecular Formula:C₂₇H₃₃Cl₂N₇O₅S
Molecular Weight:638.575
Hs Code.:

C<sub>27</sub>H<sub>33</sub>Cl<sub>2</sub>N<sub>7</sub>O<sub>5</sub>S

Synonyms:C₂₇H₃₃Cl₂N₇O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₃Cl₂N₇O₅S

Chemical Property:

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Technology Process of C₂₇H₃₃Cl₂N₇O₅S

There total 8 articles about C₂₇H₃₃Cl₂N₇O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 217806-26-3
tert-butyl N-(azetidin-3-yl)carbamate hydrochloride

: 1353628-61-1
(S)-N-(4-chloro-2-(2-(5,7-dichloropyrazolo[1,5-a]pyrimidin-2-yl)piperidine-1-carbonyl)phenyl)methanesulfonamide

: 1353629-09-0
C₂₇H₃₃Cl₂N₇O₅S

Guidance literature:: With sodium hydrogencarbonate; In water; acetonitrile; at 20 ℃; for 18h;

Reference yield:

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 1353629-09-0
C₂₇H₃₃Cl₂N₇O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h

2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C

2.2: -78 - -40 °C

2.3: -78 - 20 °C

3.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

4.1: sodium methylate / methanol / 5 h / 78 °C

5.1: trichlorophosphate / 3 h / 100 °C

6.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C

6.2: 0.67 h / 20 °C / Cooling with ice

7.1: sodium hydrogencarbonate / acetonitrile; water / 18 h / 20 °C

With oxalyl dichloride; sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium hydrogencarbonate; caesium carbonate; trichlorophosphate; In tetrahydrofuran; methanol; hexanes; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 203056-27-3
tert-butyl (2S)-2-{[methoxy(methyl)amino]-carbonyl}piperidine-1-carboxylate

: 1353629-09-0
C₂₇H₃₃Cl₂N₇O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.42 h / -78 - -20 °C / Inert atmosphere

1.2: 3.08 h / -78 - -45 °C

1.3: -78 - 20 °C

2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

3.1: sodium methylate / methanol / 5 h / 78 °C

4.1: trichlorophosphate / 3 h / 100 °C

5.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C

5.2: 0.67 h / 20 °C / Cooling with ice

6.1: sodium hydrogencarbonate / acetonitrile; water / 18 h / 20 °C

With oxalyl dichloride; sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium hydrogencarbonate; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;